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  • X-ray diffractometer (XRD) D8 ADVANCE
  • X-ray diffractometer (XRD) D8 ADVANCE

X-ray diffractometer (XRD) D8 ADVANCE

Due to its excellent adaptability, you can measure all types of samples using only D8 ADVANCE: from liquid to powder, from thin films to solid blocks.
Both novice and experienced users can easily and error free make configuration changes. This is all achieved through Brooke's unique DAVINCI design: when configuring instruments, there is no need for tools or alignment, and it is also supported by automated real-time component recognition and verification.
DetailsApplicationParameter

TWIN/TWIN optical path

Brooke's exclusive invention of TWIN-TWIN optical path design greatly simplifies the operation of D8 ADVANCE, making it suitable for various applications and sample types. For user convenience, the system can automatically switch between four different beam geometries. This system can switch between Bragg Brentano powder diffraction geometry and parallel beam geometry of poorly shaped samples, coatings, and films without the need for manual intervention. It is an ideal choice for analyzing all types of samples, including powders, bulk objects, fibers, sheets, and films (amorphous, polycrystalline, and epitaxial), in both environmental and non environmental conditions. X-ray diffractometer



Dynamic Beam Optimization (DBO)

Brooke's unique DBO function sets a new and important benchmark for the quality of X-ray diffraction data. The automatic synchronization function of motor driven divergent slits, anti scattering screens, and variable detector windows can provide you with irreplaceable data quality, especially in low 2 Ɵ At an angle. In addition, all LYNXEYE detectors support DBO: SSD160-2, LYNXEYE-2, and LYNXEYE XE-T.




LYNXEYE XE-T

LYNXEYE XE-T is the flagship product of the LYNXEYE series detectors. It is currently the only energy dispersion detector on the market that can collect 0D, 1D, and 2D data, suitable for all wavelengths (from Cr to Ag), with vertex counting rate and better angular resolution, making it an ideal choice for all X-ray diffraction and scattering applications.

LYNXEYE XE-T has an energy resolution better than 380 eV, which is truly outstanding, making it a better performing fluorescent filter detector system on the market. With it, you can filter 100% of the excited iron fluorescence with zero intensity loss, without the need for metal filters, so there are no artifacts in the data, such as residual K ß and absorption edges. Similarly, there is no need for a secondary monochromator that will remove intensity.

Brooke provides a unique LYNXEYE XE-T detector guarantee: no defects are guaranteed upon delivery!



powder diffraction

X-ray powder diffraction (XRPD) technology is one of the important material characterization tools. Many information in the powder diffraction pattern is directly derived from the atomic arrangement of the phase. In D8 ADVANCE and DIFFRAC With the support of SUITE software, you will be able to easily implement common XRPD methods:

· Identify crystalline and amorphous phases and determine sample purity

· Quantitative analysis of crystalline and amorphous phases in multiphase mixtures

· Microstructure analysis (microcrystalline size, microstrain, disorder...)

· A large amount of residual stress generated by heat treatment or manufacturing of components

· Texture (preferred orientation) analysis

· Indexing, de novo crystal structure determination, and crystal structure refinement





Analysis of distribution functions

Distribution function (PDF) analysis is an analytical technique that provides structural information of disordered materials based on Bragg and diffuse scattering ("total scattering"). Among them, you can obtain information about the average crystal structure of the material (i.e. long-range ordering) through Bragg diffraction peaks, and characterize its local structure (i.e. short-range ordering) through diffuse scattering.

In terms of analysis speed, data quality, and analysis results for amorphous, weakly crystalline, nanocrystalline, or nanostructured materials, D8 ADVANCE and TOPAS software have replaced better performing PDF analysis solutions on the market:

· Phase identification

· Structural measurement and refinement

· Nanoparticle size and shape




Thin films and coatings

The principle used for thin film and coating analysis is the same as XRPD, but further provides beam adjustment and angle control functions. Typical examples include but are not limited to phase identification, crystal quality, residual stress, texture analysis, thickness determination, and composition and strain analysis. When analyzing thin films and coatings, emphasis is placed on analyzing the characteristics of layered materials with thicknesses between nm and µ m (from amorphous and polycrystalline coatings to epitaxial growth thin films). D8 ADVANCE and DIFFRAC SUITE software can perform high-quality thin film analysis as follows:

·Grazing incidence diffraction

· X-ray reflection method

· High resolution X-ray diffraction

· Reciprocal spatial scanning


function
specifications
advantage
TRIO optical path and TWIN optical path

Software button switching:

Motor driven divergent slit (BB geometry)

Gaoqiang degree Ka1,2 parallel beam

High resolution Ka1 parallel beam

Exclusive Inventions: US10429326, US6665372, US7983389

Fully automated electric switching between up to 6 different beam geometries without the need for manual intervention

It is an ideal choice for all types of sample analysis, including powders, bulk materials, fibers, sheets, and thin films (amorphous, polycrystalline, and epitaxial)

Dynamic beam optimization

Dynamic synchronization:

Motor driven divergent slit

Motor driven anti scattering screen

Variable detector window

two Ɵ Angle range: less than 1 degree to>greater than 150 degrees

The data is almost unaffected by scattering from air, instruments, and sample racks

Improved detection lower limit, allowing for quantitative analysis of small amounts of crystalline and amorphous phases

In the smaller 2 θ Angle, with irreplaceable performance, capable of precise research on clay, drugs, zeolites, porous materials, and other materials

LYNXEYE XE-T

Energy resolution:<380 eV @ 8 KeV

Detection modes: 0D, 1D, 2D

Wavelength: Cr, Co, Cu, Mo, and Ag

Exclusive inventions: EP1647840, EP1510811, US20200033275

No need for K-filter and secondary monochromator

Copper radiation can filter iron fluorescence 100%

Speed 450 times faster than traditional detector systems

BRAGG 2D mode: Collect 2D data using divergent primary wire harnesses

Special detector guarantee: there will be no damage during delivery

EIGER2 R
A new generation detector developed by Dectris based on hybrid photon counting technology, supporting multiple modes (0D/1D/2D)

Seamless integration of 0D, 1D, and 2D detection in step scanning, continuous scanning, and advanced scanning modes

Ergonomic alignment free detector rotation function that can be optimized γ Or 2 Ɵ Angle range

Using a complete detector field of view and tool free panoramic diffraction beam optical system

Continuously variable detector positions to balance angle range and resolution

Rotating light tube
Easy and fast alignment free switching between online and spot focus applications

No need to disconnect cables or water pipes, no need to disassemble pipes

DAVINCI Design: Fully Automatic Detection and Configuration Focusing Direction

Automatic sampler

FLIPSTICK: 9 samples

AUTOCHANGER: 90 samples

Running in reflection and transmission geometry
D8 angle measuring instrument
Double circle angle measuring instrument with stepper motor and optical encoder

Brooke's unique collimation guarantee ensures irreplaceable accuracy and precision

Maintenance-free drive mechanism/gear unit, lifetime lubrication

Non environmental conditions

Temperature: from -4K to 2500K

Pressure: 10- æ mbar to 100 bar

Humidity: 5% to 95%

Conduct research under both environmental and non environmental conditions

DIFFRAC design helps you easily replace sample tables